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Extra resources for Amino Acids, Peptides and Proteins (SPR Amino Acids, Peptides, and Proteins (RSC)) (vol. 4)
R. Knorr and G. K. Staudinger, Chem. , 1971, 104, 3621, 3633. 24 Amino-acids, Peptides, and Proteins Amino-acids continue to be used as convenient chiral reagents both in synthesis and chromatography. 1°8 C. -A systematic investigation of the desulphurization of sulphur-containing amino-acids with Raney nickel has established that cysteine and cystine can be completely desulphurized under relatively mild conditions, whereas methionine is essentially ~ n c h a n g e d . lsa SAcetamido-methylcysteine can be directly oxidized to cystine derivatives with iodine,le3 and the method has been applied to the synthesis of the previously unknown cyclo-L-cystine (46).
N. Kelson, J. , 1971,59,437. J. P. Ellis, jun. and J. M. Prescott, J . , 1971,61,152. R. M. Osborne, R. W. Longton, and B. L. Lamberts, Analyt. , 1971, 44, 317. A. A. Christman, Analyt. , 1971, 39, 181. J. M. Manning, J . Biol. , 1971, 246, 2926. J. Boisseau and P. Jouan, J . , 1971, 54,231. C. Haworth and R. W. A. Oliver, Biochem. , 1971,124,255. V. A. Spivak, V. V. Shcherbukhin, V. M. Orlov, and J. M. Varshavsky, Analyt. , 1971,39,271; V. A. Spivak, V. A. Fedoseev, V. A. Orlov, and J. M. , 1971, 44, 12; V.
A. Elvidge, J. R. Jones, and E. A. Evans, Org. Magn. Resonance, 1971, lS7 L. Fowden, P. M. Scopes, and R. N. Thomas, J . Chem. (0,1971,833. E. G. Jorgensen, Tetrahedron Letters, 1971, 863. lSs lS4 138 1971, 5, 262. 3, 127. 20 Amino-acids, Peptides, and Proteins summation of the two effects leads to the cancellation of contributions in some 30" sectors and reinforcement in others, as illustrated in Figure 1. Since the carboxylate ion has a true plane of symmetry the corresponding sectors below the plane are of opposite sign.